Fardhyanti, Dewi Selvia and Damayanti, Astrilia and Imani, Nadya Alfa Cahaya and Mulyaningtyas, Akida and Setyawidianingsih, Nur Kiara and Andhini, Ageng Linda (2020) Phenolic compound separation from bio-oil produced from pyrolysis of coffee shell at 700ºc using liquid-liquid extraction. Journal of Physics: Conference Series, 1444. ISSN 1742-6596

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Abstract

Coffee shell is an agricultural waste with high lignocellulose content which potentially produces bio-oil as an environmentally alternative fuel. Bio-oil was produced from agricultural waste (biomass) using pyrolysis process that was carried out at 700°C and 1 atm. Bio-oil contains about 28.4% of caffeine, an alkaloid compounds that contains nitrogen atoms from primary metabolites of amino acids. It formed gum in the fuel oil and caused the engine damaged. Separation of phenolic compound from bio-oil was done by liquid-liquid extraction using chloroform and n-hexane as a solvent for 10, 30, 50 minutes at 30°C and stirring speed 250 rpm with feed-solvent ratio 1:4, 1:6, 1:8. The phenolic compound in the extract and raffinate phase were analyzed using UV-Vis spectrophotometer. The aim of this research is to obtain the effect of solvent, time of extraction process and feed-solvent ratio on the yield of phenolic compound. The result showed that the highest yield is 77.93% which were obtained using chloroform as solvent for 50 minutes extraction process with feed-solvent ratio of 1:8

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